微波消解-电感耦合等离子体质谱法同时测定沙棘汁饮料中18种无机元素
目的 建立微波消解-电感耦合等离子体质谱法(inductively coupled plasma mass spectrometry, ICP-MS)同时测定沙棘汁饮料中18种无机元素的方法。方法 采用微波消解法对沙棘汁饮料样品进行处理, 采用ICP-MS法测定, 对前处理过程和仪器条件进行了优化, 对方法性能进行考察, 并将该方法用于4批市售沙棘汁样品中18种元素含量的检测。结果 该方法线性范围宽, 线性关系良好(r>0.995), 精密度高, 18种元素的加标回收率为96.4%~107.3%, 相对标准偏差(relative standard deviation, RSD)为0.3%~5.9%。结论 微波消解-ICP-MS法前处理过程简单, 分析时间短, 方法快速、准确、可靠, 能够满足沙棘汁中多种元素同时检测的需要。
Objective To establish a method for simultaneous determination of 18 kinds of inorganic elements in sea-buckthorn juice by microwave digestion-inductively coupled plasma-mass spectrometry (ICP-MS). Methods The sea-buckthorn juice beverage samples were processed by microwave digestion method, then determined by ICP-MS, and the pretreatment process and instrument conditions were optimized. The performance of the method was examined, and the method was applied to detect 18 kinds of inorganic elements in 4 batches of commercially available sea-buckthorn juice samples. Results The method had a wide linear range, good linearity (r>0.995), high precision, the recoveries of 18 kinds of inorganic elements were 96.4%-107.3%, and the relative standard deviations (RSDs) were 0.3%-5.9%. Conclusion This method has a simple pretreatment process and a short analysis time. It is fast, accurate and reliable, and is suitable for simultaneous determination of various elements in sea-buckthorn juice.
标题：微波消解-电感耦合等离子体质谱法同时测定沙棘汁饮料中18种无机元素
英文标题：Simultaneous determination of 18 kinds of inorganic elements in sea-buckthorn juice by microwave digestion-inductively coupled plasma mass-spectrometry
作者：
董亚蕾 中国食品药品检定研究院
刘钊 中国食品药品检定研究院
高文超 中国食品药品检定研究院
王海燕 中国食品药品检定研究院
曹进 中国食品药品检定研究院
丁宏 中国食品药品检定研究院
中文关键词:沙棘汁,微波消解,电感耦合等离子体质谱法,无机元素,
英文关键词:sea-buckthorn juice,microwave digestion,inductively coupling plasma mass spectrometry,inorganic element,
发表日期：2018-10-16
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